{"id":6,"date":"2024-07-22T15:37:35","date_gmt":"2024-07-22T15:37:35","guid":{"rendered":"https:\/\/site.uvm.edu\/chemistry\/?page_id=6"},"modified":"2024-07-22T15:42:23","modified_gmt":"2024-07-22T15:42:23","slug":"user-guides-for-bruker-nmr-spectrometer","status":"publish","type":"page","link":"https:\/\/site.uvm.edu\/chemistry\/user-guides-for-bruker-nmr-spectrometer\/","title":{"rendered":"User Guides for Bruker NMR spectrometer"},"content":{"rendered":"\n

Here are some user guides that will help you with NMR data acquisition on UVM\u2019s Bruker NMR spectrometer.  Please e-mail Monika<\/a> to request training OR to get help with some of the more complicated experiments.<\/p>\n\n\n\n

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  1. For a basic introduction to acquiring 1H and 13C 1D data\u00a0see this guide<\/a>. (Bruker Speedy Setup Guide_v.1.5.pdf)<\/li>\n\n\n\n
  2. If you\u2019d like to acquire 19F data\u00a0see this guide<\/a>. (Bruker-19F1Dacquisition.pdf)<\/li>\n\n\n\n
  3. And if you\u2019d like to acquire 29Si data\u00a0see this guide<\/a>. (Bruker-29Si1Dacquisition.pdf)<\/li>\n\n\n\n
  4. Determining T1 relaxation values for different 1Hs in your sample is simple.\u00a0Please\u00a0see this guide<\/a>\u00a0for doing it on the Bruker NMR (Bruker-T1estimates.pdf).<\/li>\n\n\n\n
  5. For selective 1D experiments, be it NOESY or TOCSY or a variety of others,\u00a0see this guide<\/a>\u00a0for help (Bruker-Selective1Dexperiments.pdf).<\/li>\n\n\n\n
  6. If you need to do Variable Temperature (VT) experiments, you should get Monika\u2019s help with this, because depending on whether you want to go hot (easier) or cold (more complicated) there are several steps in the process.\u00a0 See the\u00a0Bruker VT guide<\/a>\u00a0for this (Bruker-VTexperiments.pdf)<\/li>\n\n\n\n
  7. Now for solid state NMR experiments, you will need to let Monika know at least a month ahead of time.\u00a0 The probe gets installed infrequently, liquids users need to be notified and the installation is a fairly complicated process.\u00a0This solid state NMR guide<\/a>\u00a0will help you with acquiring solids data (Bruker-SolidState-NMR-data-acquisition.pdf)<\/li>\n<\/ol>\n\n\n\n

    User guides for Varian NMR spectrometer:<\/h2>\n\n\n\n

    The following user guides will help you with acquiring data on our Varian NMR spectrometer.  Please e-mail Monika<\/a> to schedule a training or get help.<\/p>\n\n\n\n

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    1. For a basic introduction to acquiring 1H 1D spectra\u00a0see this guide<\/a>\u00a0(Varian-1D-DataAcquisition.pdf).<\/li>\n\n\n\n
    2. If you\u2019d like to acquire 2D spectra on the Varian,\u00a0see this guide<\/a>\u00a0(Varian-2D-experiment-setup_v1.0.pdf)<\/li>\n<\/ol>\n","protected":false},"excerpt":{"rendered":"

      Here are some user guides that will help you with NMR data acquisition on UVM\u2019s Bruker NMR spectrometer.  Please e-mail Monika to request training OR to get help with some of the more complicated experiments. User guides for Varian NMR spectrometer: The following user guides will help you with acquiring data on our Varian NMR spectrometer.  Please e-mail … <\/p>\n

      Continue reading “User Guides for Bruker NMR spectrometer”<\/span><\/a><\/p>\n","protected":false},"author":9477,"featured_media":0,"parent":0,"menu_order":0,"comment_status":"closed","ping_status":"closed","template":"","meta":{"footnotes":""},"class_list":["post-6","page","type-page","status-publish","hentry","entry"],"featured_image_src":null,"featured_image_src_square":null,"_links":{"self":[{"href":"https:\/\/site.uvm.edu\/chemistry\/wp-json\/wp\/v2\/pages\/6","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/site.uvm.edu\/chemistry\/wp-json\/wp\/v2\/pages"}],"about":[{"href":"https:\/\/site.uvm.edu\/chemistry\/wp-json\/wp\/v2\/types\/page"}],"author":[{"embeddable":true,"href":"https:\/\/site.uvm.edu\/chemistry\/wp-json\/wp\/v2\/users\/9477"}],"replies":[{"embeddable":true,"href":"https:\/\/site.uvm.edu\/chemistry\/wp-json\/wp\/v2\/comments?post=6"}],"version-history":[{"count":3,"href":"https:\/\/site.uvm.edu\/chemistry\/wp-json\/wp\/v2\/pages\/6\/revisions"}],"predecessor-version":[{"id":18,"href":"https:\/\/site.uvm.edu\/chemistry\/wp-json\/wp\/v2\/pages\/6\/revisions\/18"}],"wp:attachment":[{"href":"https:\/\/site.uvm.edu\/chemistry\/wp-json\/wp\/v2\/media?parent=6"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}